Hach AN-ISE sc Addendum To The Operator Manual

DOC023.98.90594

AN-ISE sc, AISE sc, NISE sc probe

Addendum—Operation with the SC1500 Controller

05/2017, Edition 1

3

Table of contents

English..................................................................................................................................................... 5

Deutsch.................................................................................................................................................. 23

Español.................................................................................................................................................. 41

Français ................................................................................................................................................. 59

Italiano ................................................................................................................................................... 79

Nederlands ............................................................................................................................................ 97

Dansk ................................................................................................................................................... 115

Polski ................................................................................................................................................... 133

4

Table of contents

English 5

Section 4 Operation

English

For more information on System Setup (current outputs, relays, and

network interfaces), refer to the sc1500 User Manual.

The following tables show the sensor menu for the AN-ISE sc

probe, AISE sc probe and NISE sc probe. If a menu item does not

apply to all three probes, its applicability is explained in footnotes.

Footnote

1 indicates applicability to the AN-ISE sc probe. The

AN-ISE sc probe is used to determine the ammonium and nitrate

concentration, as well as the potassium and chloride concentration.

Footnote

2 indicates applicability to the AISE sc probe. The AISE sc

probe is used to determine the ammonium and potassium

concentration.

Footnote

3 indicates applicability to the NISE sc probe. The NISE sc

probe is used to determine the nitrate concentration and chloride

concentration.

4.1 Sensor diagnostics menu

SENSOR STATUS

AN-ISE sc or AISE sc or NISE sc

Error list Shows all current error messages.

Warning list Shows all current warnings.

4.2 Sensor setup menu

SELECT AN-ISE sc or AISE sc or NISE sc (if more than one sensor or analyzer is attached)

Calibration

Matrix correction

Matrix correction options.

The most recently used menu is displayed.

The currently active corrections are shown in Information.

None No Matrix corrections activated

1-point matrix correction 1-point matrix correction

NH

4

+ NO

3

1

1-point matrix correction for ammonium and nitrate

NH

4

1,2

1-point matrix correction for ammonium

NO

3

1,3

1-point matrix correction for nitrate

NH

4

+ K

1,2

1-point matrix correction for ammonium and potassium

NO

3

+ Cl

1,3

1-point matrix correction for nitrate and chloride

NH

4

+K + NO

3

+Cl

1

1-point matrix correction for ammonium, potassium, nitrate and chloride

Take the grab sample

immediately for the lab

analysis.

Information window: When this window appears, the sample must be taken immediately

and then analyzed in the laboratory.

1-point value correction

Perform 1-point value correction.

The most recently used menu is displayed.

The currently active corrections are shown in Information.

NH

4

–N

1

Select parameter for the 1-point value correction

NO

3

–N

1

Enter the values for the

first point

Enter the values for the 1-point value correction

Note: The following example shows the input when using a AN-ISE sc probe for

ammonium. When using the AISE sc probe, the input is the same. When using the

NISE sc, it is only possible to input the nitrate and chloride values.

6 English

Operation

Calibration (continued)

AN-ISE SC NH

4

–N Enter the displayed ammonium value

AN-ISE SC K Enter the displayed potassium value

Lab value NH

4

–N Enter the laboratory ammonium value

Confirm the entry. Confirm the values entered

Correction result Display the correction results

2-point value correction Perform 2-point value correction

NH

4

–N

1

Select parameter for the 2-point value correction

NO

3

–N

1

Enter the values for the

first point

Enter the values for the 2-point value correction (first point)

Note: The following example shows the input when using a AN-ISE sc probe for

ammonium. When using the AISE sc probe, the input is the same. When using the

NISE sc, it is only possible to input the nitrate and chloride values.

AN-ISE SC NH

4

–N Enter the displayed ammonium value

AN-ISE SC K Enter the displayed potassium value

Lab value NH

4

–N Enter the laboratory ammonium value

Confirm the entry. Confirm the values entered

Enter the values for the

second point.

Enter the values for the 2-point value correction (second point).

Note: The following example shows the input when using a AN-ISE sc probe for

ammonium. When using the AISE sc probe, the input is the same. When using the

NISE sc, it is only possible to input the nitrate and chloride values.

AN-ISE SC NH

4

–N Enter the displayed ammonium value

AN-ISE SC K Enter the displayed potassium value

Lab value NH

4

–N Enter the laboratory ammonium value

Confirm the entry. Confirm the values entered

Correction result Display the correction results

More corrections Other matrix correction options

None No More corrections is activated

2-point matrix correction A 2-point matrix correction can be performed here

NH

4

1

Parameter selection for the 2-point matrix correction.

NO

3

1

Concentration

measurement 1

Saves the currently measured measurement for the first point

Date Displays the date of the current correction of the first point

Concentration 1 Entry and display of reference value for the first point

Concentration

measurement 2

Saves the currently measured measurement for the second point

Date Displays the date of the current correction of the second point

Concentration 2 Entry and display of the reference value for the second point

Previous corrections Selection of one of the last corrections performed

Sensor code The sensor code can be activated or entered here

Activate Activates the sensor code for the individual channels

NH

4

+ K

1

Activate the sensor code for ammonium and potassium

NO

3

+ Cl

1

Activate the sensor code for nitrate and chloride

NH

4

+K + NO

3

+Cl

1

Activate the sensor code for ammonium, potassium, nitrate and chloride

Reset calibration Activates factory calibration

4.2 Sensor setup menu (Continued)

English 7

Operation

Calibration (continued)

Sensor code Entry of the sensor code

Lab value correction The laboratory values of the last matrix correction can be changed

Enter the lab value.

Enter the laboratory values if 1-point matrix correction or 2-point matrix correction has

been selected

Ammonium

1,2

Entry of ammonium laboratory value

Nitrate

1,3

Enter the laboratory value for nitrate

Potassium

1,2

Enter the laboratory value for potassium

Chloride

1,3

Enter the laboratory value for chloride

Confirm the entry. Confirm the values entered

Correction result Display the correction results

NH

4

–N

1,2

Displays whether or not the ammonium correction was successful

NO

3

–N

1,3

Shows whether or not the nitrate correction was successful

K+

1,2

Displays whether or not the potassium correction was successful

Cl

1,3

Displays whether or not the chloride correction was successful

Information Information on the matrix correction used per parameter

NH

4

–N

1,2

Matrix correction used for ammonium

NO

3

–N

1,3

Matrix correction used for nitrate

K+

1,2

Matrix correction used for potassium

Cl

1,3

Matrix correction used for chloride

Settings

Name

Enter or edit the name.

Up to 10 alphanumeric characters

Unit Select either mg/L or ppm as the measurement unit

Parameter Select NH

4

–N or NH

4

and/or NO

3

–N or NO

3

Temperature Selection of °C or °F as temperature unit

Offset temperature Enter a temperature offset

Response time Entry of the response time (30 sec to 300 sec)

Datalog interval

Select the data log interval (OFF, 30 sec, 1 min, 2 min, 5 min, 10 min, 15 min and

30 min), 5 min is the factory setting

K+ compensation

1,2

Select automatic potassium compensation:

On

Off

0 = compensation OFF

0.1–2000 mg/L Cl = Fixed compensation value

K+ concentration

1,2

Only shown when K+ COMPENSATE is OFF

Cl - compensation

1,3

Select automatic chloride compensation:

On

Off

0 = compensation OFF

0.1–2000 mg/L Cl = Fixed compensation value

Cl - concentration

1,3

Only shown when Cl COMPNSATE is OFF

Reset configuration Resets the configuration to the factory setting

Maintenance

Sensor information Information on the connected sensor

Sensor type Name of the connected sensor

4.2 Sensor setup menu (Continued)

8 English

Operation

Maintenance (continued)

Name Serial number or name of the measurement location

Serial number Serial number of the connected sensor

Sensor type Instrument designation of the connected sensor

Software Software version

Calibration history

Data of the selected matrix correction and information about slope and offset of the

individual channels, for example

NH

4

–N

1,2

Matrix correction selected for ammonium

NO

3

–N

1,3

Matrix correction selected for nitrate

K+

1,2

Matrix correction selected for potassium

Cl

1,3

Matrix correction selected for chloride

Signals Signals and measurement results of the individual measurement channels

Ammonium

1,2

Display the signals and measurement results for ammonium

Nitrate

1,3

Shows the signals and measurement results for nitrate

Potassium

1,2

Display the signals and measurement results for potassium

Chloride

1,3

Display the signals and measurement results for chloride

Reference electrode Displays the signals and measurement results for the reference system

mV RAW Display the signals and measurement results for MV RAW

Impedance status Display the signals and measurement results for impedance

Temperature Display the signals and measurement results for temperature

Moisture Display the signals and measurement results for humidity

RFID Display the signals and measurement results for RFID

Last calibration Shows the age of the last matrix correction

Ammonium

1,2

Display the age of the last matrix correction for ammonium

Nitrate

1,3

Display the age of the last matrix correction for nitrate

Service

Cartridge test Perform a sensor check with the test cartridge

Cartridge test Display whether the individual sensor channels are OK or not

Maintenance Displays whether or not DIAG/TEST is OK

Ground rod Displays whether or not GNDROD is OK

Reference electrode Displays whether or not REF channel is OK

NO

3

1,3

Displays whether or not NO3 channel is OK

NH

4

1,2

Displays whether or not NH4 channel is OK

ORP Displays whether or not ORP channel is OK

Cl-

1,3

Shows whether or not Cl channel is OK

K+

1,2

Displays whether or not K channel is OK

Temperature Displays whether or not temperature channel is OK

Cartridge replacement Follow the menu process

Cleaning... Follow the menu process

1

Applies to AN-ISE sc

2

Applies to AISE sc

3

Applies to NISE sc

4.2 Sensor setup menu (Continued)

English 9

Operation

4.3 Calibration/matrix correction

The four electrodes with the reference system of the compact

sensor cartridge were calibrated with one another at the factory

using special standard solutions (CARTICAL

TM

). However, the

membranes on the ion-selective electrodes are not 100% selective

due to other substances that may affect the measurement. Perform

a matrix correction (refer to 4.3.4, page 11) to compensate for other

ions present on the ISE electrodes.

Potassium has the largest interference effect on the ammonium

membrane, while chloride has the largest effect on the nitrate

membrane. The AN-ISE sc probe compensates for this problem

with the aid of a built-in potassium/chloride electrode.

When using the AISE sc probe, only the ammonium membrane and

the integrated potassium electrode are active.

When using the NISE sc probe, only the nitrate membrane and the

integrated chloride electrode are active.

Cross sensitivities between ammonium and potassium/nitrate are

automatically eliminated. Solids do not interfere with the

measurement. Due to matrix effects, correction and validation

cannot be performed with standard solutions. A matrix correction

can be carried out quickly and easily at any time.

4.3.1 Sensor code calibration

The sensor code is a calibration code and is delivered with the

sensor cartridge certificate. It contains the factory calibration

described in section 3.12, page 9 for the sensor cartridge.

Instruments with automatic sensor code recognition

(LXG440.99.x000x) read this automatically and assume the

Cartrical calibration.

Instruments without automatic sensor code recognition

(LXG440.99.x001x) require the sensor code to be entered during

the initial setup and whenever a new sensor cartridge is activated. If

the sensor code certificate has been lost, carry out factory

calibration (under the sensor code menu) as a temporary solution.

After activating the code, the sensor is fully calibrated but not yet

adapted to the specific matrix of the relevant application on a waste

water treatment plant. At least 12 hours must elapse before a

matrix correction is performed to allow the cartridge to adapt to the

specific matrix.

NOTICE

A matrix correction may only be performed if the sensor has been

immersed in the corresponding waste water matrix for over 12 hours.

This is the minimum time required to adapt the ISE membranes to the

waste water matrix.

10 English

Operation

Proceed as follows to change the sensor code:

1. Select

SENSOR MENU > AN-ISE SC or AISE SC or NISE SC >

CALIBRATION > MORE CORRECTIONS> SENSOR CODE >

ENTER

2. Enter the sensor code.

3. Press

ENTER to confirm and activate the sensor code. The day

meter for the cartridge is set to zero.

All old calibration data are now overwritten with the new calibration

data from the sensor code. The sensor code data is checked by the

system. If an error is indicated, check the sensor code and, if

necessary, enter the sensor code again.

4.3.2 Matrix correction via LINK2SC

The LINK2SC procedure offers a secure method of data exchange

between process probes and LINK2SC-compatible photometers

using an SD memory card or via a local area network (LAN). Two

different options are available:

a. The pure laboratory control measurement

b. A matrix correction that involves the measurement data

generated in the laboratory being used to correct the probe

During a pure control measurement, the measurement data is

transferred from the probe to the photometer where it is then

archived together with the photometric reference data that has

been recorded.

During a matrix correction, the reference data generated in the

laboratory is transferred to the probe to be used for the correction.

The matrix correction process requires operating steps to be

completed on the sc controller and on a LINK2SC-compatible

photometer.

Refer to the LINK2SC user manual for a detailed description of the

LINK2SC procedure.

When using the LINK2SC software, sections 4.3.3 and 4.3.4 are

not relevant.

4.3.3 Matrix correction – manual

ISE probes offer different options (refer to Table 1) for correcting

the sensor value with laboratory values (as a reference value).

The laboratory value of the water sample is entered as nitrate

nitrogen (NO

3

–N) and/or as ammoniacal nitrogen (NH

4

–N). This

laboratory value replaces the prior value measured by the sensor.

English 11

Operation

4.3.4 Performing the matrix correction

Note: Take laboratory value measurements or reference values promptly

or, alternatively, take these from the stabilized sample. This will prevent

changes in sample concentration, as time is a factor in comparative tests.

Refer to 7.3 Validation accessories, Page 39 for recommended

laboratory measurement tests.

4.3.4.1 1-point matrix correction

Proceed as follows to perform 1-point matrix correction:

1. Select

SENSOR MENU > AN-ISE SC or AISE SC or NISE SC >

CALIBRATION > 1-point matrix correction

.

2. Select

2-point matrix correction from the selection window and

press

ENTER.

3. Select the parameters you wish to correct and confirm by

pressing

ENTER.

Selection options for AN-ISE sc:

NH

4

+ NO

3

; NH

4

; NO

3

; NH

4

+ K; NO

3

+ Cl; NH

4

+ K NO

3

+ Cl

Selection options for AISE sc:

NH

4

; NH

4

+ K

Table 1 Correction options for ISE probes

Correction option Application

1-point matrix

correction

A 1-point matrix correction is the most commonly used correction option and performs a 1-point

matrix correction for ammonium and/or nitrate (4.3.4.1, page 11). It is advisable to perform a 1-point

matrix correction as the first correction. The 1-point matrix correction can be performed both with

and without correction of the compensation electrodes (potassium or chloride); in most cases, it is

sufficient to perform it without correction. A correction featuring potassium and/or chloride is only

necessary if a high level of accuracy is required. With a 1-point matrix correction, a sample must be

taken when the correction is triggered and analyzed in the laboratory. The 1-point matrix correction is

activated when the laboratory value is entered.

1-point value

correction

1-point value correction (correction at one concentration point) corresponds to a 1-point matrix

correction with an alternative entry format.

Comparison values between the ISE probe and the laboratory can be collected over a period of

around a week with this correction. The correction can be performed at a later stage.

2-point value

correction

2-point value correction (correction at 2 different concentration points) should be performed if

dynamic concentration fluctuations are present over at least half a decade

1

and a 2-point

matrix correction or 1-point value correction does not achieve a sufficiently accurate result.

Comparison values between the ISE probe and the laboratory can be collected over a period of

around a week with this correction. The correction can be performed at a later stage.

2-point matrix

correction

The 2-point matrix correction corresponds to a 2-point value correction, but uses an

alternative entry format and is recommended if there is a dynamic process with a large

nitrate/ammonium fluctuation greater than at least half a decade

1

. With a 2-point matrix correction, a

sample must be taken for both points when the correction is triggered and analyzed in the laboratory.

The 2-point matrix correction is activated when the laboratory value is entered.

Previous corrections

Return to one of the last matrix and value corrections performed if a correction has not produced

a successful result.

1

Examples of half a decade: The concentration of nitrogen nitrate shifts between 1 and 5 mg NO

3

–N or

between 5 and 25 mg/L NO

3

–N. (conc2 = (conc1 x 10)/2)

Calibration

Matrix correction

More corrections

Information

12 English

Operation

Selection options for NISE sc:

NO

3

; NO

3

+ Cl

The sensor saves the current values of the selected parameters at

this point.

4. Take a water sample immediately from the closest point

possible to the sensor. Filter the sample as quickly as possible

and carry out a prompt laboratory analysis of the selected

parameters, as the measurement value can change quickly.

When the laboratory value has been determined, proceed as

follows:

5. Select SENSOR MENU > AN-ISE SC or AISE SC or NISE SC

> CALIBRATION > Enter the lab value.

6. The laboratory values for the parameters can only be entered if

the 1-point matrix correction correction has been selected

beforehand. Once the laboratory values have been entered,

select Confirm the entry. to confirm.

When the entered laboratory value is confirmed, the matrix

correction is activated.

7. Once the correction is activated, the result Correction result is

shown.

Note: This process must always be carried out in full to make sure the

matrix correction is completed successfully.

If a correction does not produce a successful result, calculations are made

with the previous correction.

4.3.4.2 1-point value correction

The 1-point value correction offers the option of retrospectively

performing a matrix correction at one point.

1. Take several samples with different concentrations on various

days, preferably within one week. Analyze the samples in the

laboratory. During the time the samples are being taken, the

sample temperature should vary a maximum of 5 °C, as

temperature changes are not taken into account in the value

correction.

2. Make a note of the two values measured in the samples and

displayed for the parameters to be corrected (ammonium and

potassium values, or nitrate and chloride values)

3. Also note the laboratory values measured for ammonium or

nitrate.

These three values form the correction point.

4. From the values taken, select a correction point that lies in the

middle of the expected concentration range.

1-point matrix

correction

Take the grab sample

immediately for the lab

analysis.

Calibration

Matrix correction

More corrections

Enter the lab value.

Information

Calibration

Matrix correction

More corrections

Information

English 13

Operation

5. Go to the sensor menu and select CALIBRATION > MATRIX

CORRECTION >

1-point value correction and confirm by

pressing

ENTER.

6. Select the parameter1 (NH

4

–N or NO

3

–N) that requires

correction.

Note: The example opposite shows the NH

4

-N and K correction of the

AN-ISE sc probe.

7. Enter the three values for the sought correction point and push

Confirm the entry. to activate the correction.

Correction result is shown.

Note: If a correction does not produce a successful result, calculations are

made with the previous correction.

After successful completion of value correction, the corrected value is

shown as the display value for ammonium or nitrate the next time the menu

is opened.

4.3.4.3 2-point value correction

The 2-point value correction makes it possible to perform a

subsequent 2-point correction to achieve higher accuracy for a

larger concentration range.

Note: The 2-point value correction and 2-point matrix correction are

comparable from a calculation perspective.

1. Take several samples on various days with different

concentrations, preferably within a week, and perform an

analysis of the samples in the laboratory. During the time the

samples are being taken, the sample temperature should be

around a maximum of 5 °C, as temperature changes are not

taken into account in the value correction.

Note: The 2-point matrix correction concentrations should be within a

range greater than half a decade. The following formula can assist in the

calculation of the half decade:

2. Make a note of the two values measured with the sensor in the

samples and displayed for the parameters to be corrected

(ammonium and potassium values, or nitrate and chloride

values).

3. Also note the laboratory value measured for ammonium or

nitrate.

All three values form one of the two correction points.

4. Look for two correction points where the laboratory values are

at least half a decade apart and display typical operating

conditions for the installation.

Enter value point

AN–ISE SC NH

4

–N

AN–ISE SC K

Lab value NH

4

–N

Confirm the entry.

1Applies to AN-ISE sc

Calibration

Matrix correction

More corrections

Information

Conc2 >=

Conc1 x 10

2

14 English

Operation

5. Go to the sensor menu and select CALIBRATION > MATRIX

CORRECTION >

2-point value correction and confirm with

ENTER.

6. Select the parameter

1

(NH

4

–N or NO

3

–N) that requires

correction.

Note: When using the AN-ISE sc probe, you can only correct one

parameter at a time. If both parameters need to be corrected, the

procedure must be performed again.

7. Enter the three values for the first correction point and push

CONFIRM THE ENTRY.

Note: The example opposite shows the NH

4

-N and K correction of the

AN-ISE sc probe.

8. To activate the correction, enter the three values for the second

correction point and push

CONFIRM THE ENTRY.

Correction result is shown.

Note: If a correction does not produce a successful result, calculations are

made with the previous correction. After successful completion of value

correction, the corrected value is shown as the display value for ammonium

or nitrate the next time the menu is opened.

4.3.4.4 2-point matrix correction

Proceed as follows to perform 2-point matrix correction:

1. Select

SENSOR MENU > AN-ISE SC or AISE SC or NISE SC >

CALIBRATION > MORE CORRECTIONS

.

2. Select 2-point matrix correction from the selection window

and press

ENTER.

3. Select the Parameter requiring a 2-point matrix correction.

4. Select the point to be corrected.

5.

SELECT Concentration measurement 1 or Concentration

measurement 2

6. Take a water sample from the closest point possible to the

sensor. Filter this sample promptly and perform an immediate

laboratory analysis of the selected parameters. The

measurement value can change very quickly:

When the laboratory value has been determined, proceed as

follows:

7. Select

SENSOR MENU > AN-ISE SC or AISE SC or NISE SC >

CALIBRATE > MORE CORRECTIONS>

2-point matrix

correction

8. Select the parameters to be corrected with the laboratory value

entry:

Enter the values for the

first point

AN–ISE SC NH

4

–N

AN–ISE SC K

Lab value NH

4

–N

Confirm the entry.

Enter the values for the

second point

AN–ISE SC NH

4

–N

AN–ISE SC K

Lab value NH

4

–N

Confirm the entry.

Ammonium

Concentration

measurement 1

Date

Enter the lab value 1.

Concentration

measurement 2

Date

Enter the lab value 2.

English 15

Operation

9. Enter the laboratory reference value and confirm.

The 2-point matrix correction is activated when the entry is

confirmed for both points.

16 English

Section 5 Maintenance

5.3 Replace the sensor cartridge

The sensor cartridge is replaced as described below and in

Figure 15 on page 17.

1. Replace the cartridge using menu item

AN-ISE SC or AISE SC or NISE SC > MAINTENANCE > SERVICE >

CARTRIDGE REPLACEMENT

.

2. Clean the probe and thoroughly dry the sensor cartridge and

probe adapter.

3. Loosen the 4 socket head screws.

.

4. Pull the sensor cartridge out of the probe adapter and discard

the old sensor cartridge as per the applicable regulations.

5. Make sure that a new black gasket is installed every time the

sensor cartridge is replaced. Before the gasket is installed,

clean the surface that faces the cartridge and the groove for the

gasket.

6. Insert the new sensor cartridge into the probe adapter. Observe

the marker hole on the sensor cartridge flange and the probe

adapter.

7. Secure the sensor cartridge with the 4 socket head screws.

8. The sensor code (calibration data) is automatically read for

instruments with automatic recognition (LXG440.99.x000x). For

instruments with non-automatic recognition

(LXG440.99.x001x), enter the new sensor code manually (refer

to certificate).

NOTICE

The sensor cartridge must point downward such that no water can run into

the probe adapter. Pay attention to the contacts between the probe and

the sensor cartridge. These contacts must remain dry.

English 17

Maintenance

Figure 15 Replace the sensor cartridge

1 Socket head screw 5 Union nut

2 Sensor cartridge 6 Marker hole

3 O-ring 7 Socket head wrench

4 Sensor

18 English

Section 6 Troubleshooting

6.1 Error messages

If the sensor is in an error state, the measurement value for this

sensor will flash on the display and the relay contacts and current

outputs associated with this sensor will be stopped. The errors are

described in Table 2.

Table 2 Error messages

Displayed errors Cause Resolution

NH

4

mV is out of range!

1,2

Ammonium mV value exceeds the measurement range

Refer to 6.3.1 Troubleshooting

during operation, Page 21.

K+ mV is out of range!

1,2

Potassium mV value exceeds the measurement range

NO

3

mV is out of range!

1,3

Nitrate mV value exceeds the measurement range

Cl- mV is out of range!

1,3

Chloride mV value exceeds the measurement range

Reference electrode 1

mV is out of range!

REF1 reference value is out of measuring range

Reference electrode 2

mV is out of range!

ORP electrode mV value is out of measuring range

Temperature is out of

range!

Temperature value exceeds measurement range

No cartridge was found. No sensor cartridge connected

Connect the sensor cartridge;

refer to section 3.3, page 15.

Sensor code Sensor code calibration failed

Refer to 6.3.2 Troubleshooting

during calibration, Page 22

Humidity Humidity in the probe Inform service engineer

NH

4

-N concentration is

high.

1,2

Ammonium concentration value exceeds measuring range

Refer to 6.3.1 Troubleshooting

during operation, Page 21.

NH

4

-N concentration is

low.

1,2

Ammonium concentration value is below measuring range

NO

3

-N concentration is

high.

1,3

Nitrate concentration value exceeds measurement range

NO

3

-N concentration is

low.

1,3

Nitrate concentration value is below measurement range

K+ concentration is high.

1,2

Potassium concentration value exceeds measuring range

K+ concentration is low.

1,2

Potassium concentration value is below measuring range

Cl- concentration is high.

1,3

Chloride concentration value exceeds measuring range

Cl- concentration is low.

1,3

Chloride concentration value below measurement range

1

Applies to AN-ISE sc

2

Applies to AISE sc

3

Applies to NISE sc

English 19

Troubleshooting

6.2 Warnings

In the event of a sensor warning, all menus, relays and outputs

continue to function as normal but a warning symbol lights up.

Warnings may be used to activate a relay; users can set warning

levels to define the severity. Warnings are defined in Table 3.

Table 3 Warnings

Displayed warnings Cause Resolution

RFID data Cartridge faulty, read process failed

Replace cartridge, check probe

with test cartridge

NH

4

mV is out of range!

1,2

Ammonium mV value is close to measuring range limit

Refer to 6.3.1 Troubleshooting

during operation, Page 21.

K+ mV is out of range!

1,2

Potassium mV value is close to measuring range limit

NO

3

mV is out of range!

1,3

Nitrate mV value is close to measurement range limit

Cl- mV is out of range!

1,3

Chloride mV value is close to measurement range limit

Reference electrode 1

mV is out of range!

1st reference value is close to limit

Reference electrode 2

mV is out of range!

2nd reference value is close to limit

Temperature is out of

range!

Temperature is close to limit

The cartridge has

expired.

Sensor cartridge more than 1 year old Replace the sensor cartridge

NH

4

-N concentration is

high.

1,2

Ammonium concentration value exceeds measuring range

See 6.3.1 Troubleshooting during

operation, Page 21.

NH

4

-N concentration is

low.

1,2

Ammonium concentration value is below measuring range

NO

3

-N concentration is

high.

1,3

Nitrate concentration value exceeds measuring range

NO

3

-N concentration is

low.

1,3

Nitrate concentration value is below measurement range

K+ concentration is high.

1,2

Potassium concentration value exceeds measuring range

K+ concentration is low.

1,2

Potassium concentration value is below measuring range

Cl- concentration is high.

1,3

Chloride concentration value exceeds measuring range

Cl- concentration is low.

1,3

Chloride concentration value is below measurement range

20 English

Troubleshooting

Ammonium

1,2

Refer to 6.3.2 Troubleshooting

during calibration, Page 22.

Offset Ammonium offset exceeds measurement range

Slope Ammonium slope exceeds measurement range

Potassium

1,2

Offset Potassium offset exceeds measurement range

Slope Potassium slope is out of measuring range

Nitrate

Offset Nitrate offset is out of measurement range

Slope Nitrate slope is out of measurement range

Chloride

Offset Chloride offset is out of measurement range

Slope Chloride slope is out of measurement range

1

Applies to AN-ISE sc

2

Applies to AISE sc

3

Applies to NISE sc

Table 3 Warnings

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Hach AN-ISE sc Addendum To The Operator Manual

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Hach AN-ISE sc Addendum To The Operator Manual

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